Tandem µ-Reactor

The Frontier Lab Tandem μ-Reactor was developed to rapidly screen laboratory-prepared catalysts.
The reactor consists of a pyrolysis furnace and a catalytic reactor, and it can be directly connected to a gas chromatograph mass spectrometer (GC/MS) to observe real-time changes of the products formed by the gas-phase catalytic reaction between the sample and the catalyst.
In addition, it has a rapid heating and cooling function, and the catalyst reaction tube packed with the catalyst can be replaced within a few minutes, greatly improving the efficiency of catalyst screening. A flow controller is provided standard, allowing you to easily switch among three different reaction gases. Further, in combination with Selective Sampler and MicroJet Cryo-Trap options, automated analysis of products formed in up to eight temperature zones can be performed.

Features:

  • Catalyst reaction products can be monitored through online-MS analysis mode. Also, GC/MS analysis can be performed at desired reactor temperatures
  • Micro-Reactors capable of rapid heating/cooling The micro-Reactors feature with multi-linear temp. programs and multi-stepwise temp. programs (up to 8 steps). The ramp rate can be set from 1 ºC to maximum 200 ºC/min, while the temperature can be controlled from 40 ºC to 700 ºC
  • Rapid switching of catalyst reaction tubes: switching catalysts can be accomplished in a few minutes using the proprietary quartz reaction tube (i.d. 3 mm, o.d. 4 mm, length 78 mm)
  • In the Tandem µ-Reactor, two reactors (1st and 2nd), are individually temperature-controlled The 1st Reactor (upper reactor) is used to preheat a gas, vaporize a liquid, or thermally decompose organic solids (biomass analysis) to generate gases. The catalyst reaction tube is packed with a catalyst and placed in the 2nd Reactor (lower reactor).

Specifications:

  • Pyrolysis furnace (1st Reactor)
    • Reactor: Temperature control range: -40 to 700 ºC (1 ºC step, stainless steel pyrolysis tube), 40 to 900 ºC (1 ºC step, quartz pyrolysis tube)
    • Temperature control modes: Isothermal, linear, and stepwise temperature rise
    • Interface temperature control range: -40 ~ 400 ºC (1 ºC step)
  • Catalytic reactor (2nd Reactor)
    • Reactor: Temperature control range -40 ~ 700 ºC (1 ºC step)
    • Temperature control mode Isothermal, linear, and stepwise temperature rise
    • Interface temperature control range: -40 ~ 400 ºC (1 ºC step).

SRA Instruments S.R.L.

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